Table 2 System suitability
Replicate | Flow (1.0 mL) Buffer 80% First analyst Day—1 Column—1 | Flow (0.9 mL) | Flow (1.1 mL) | Buffer (82.5%) | Buffer (77.5%) | Second analyst | Day—2 | Column—2 | Column—3 |
|---|---|---|---|---|---|---|---|---|---|
Weight(g)/100Â mL | 0.01094 | 0.01094 | 0.01094 | 0.01092 | 0.01094 | 0.01091 | 0.01095 | 0.01097 | 0.01091 |
1 | 3744.7 | 4138.2 | 3443 | 3779.1 | 3517.1 | 3734.7 | 3794.2 | 3864.8 | 3765.9 |
2 | 3746.1 | 4115.3 | 3441.3 | 3756.2 | 3486 | 3735.2 | 3782.9 | 3896.9 | 3781.2 |
3 | 3730.9 | 4164.9 | 3434.5 | 3784.0 | 3513.5 | 3741.6 | 3846.9 | 3908.0 | 3806.3 |
4 | 3785.2 | 4155.2 | 3444.2 | 3784.5 | 3515.4 | 3722.9 | 3794.1 | 3905.9 | 3799.9 |
5 | 3791.3 | 4128.8 | 3435.8 | 3754.8 | 3554.2 | 3723.5 | 3759.1 | 3887.8 | 3796.6 |
6 | 3753.8 | 4133.0 | 3429.5 | 3754.7 | 3524.5 | 3747.1 | 3737.3 | 3904.3 | 3859.8 |
Mean P.A | 3758.7 | 4139.2 | 3438.1 | 3768.9 | 3518.5 | 3734.2 | 3785.8 | 3894.6 | 3801.6 |
STDV | 24.2 | 18.1 | 5.7 | 15.1 | 21.9 | 9.6 | 37.3 | 16.4 | 32.0 |
RSD | 0.64 | 0.44 | 0.17 | 0.40 | 0.62 | 0.26 | 0.98 | 0.42 | 0.84 |
Tailing | 1.15979 | 1.20087 | 1.15984 | 1.14816 | 1.08537 | 1.11781 | 1.11781 | 1.08023 | 0.93333 |
Plates | 5411 | 5700 | 4864 | 6078 | 4915 | 5179 | 5179 | 5135 | 5017 |