2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | ||
---|---|---|---|---|---|---|---|---|---|
Melting point (oC) | Found | 100–102 | 122–124 | 172–174 | 140–142 | 104–106 | 222–224 | 138–140 | 160–162 |
Lit* | 100–102 | 120–122 | 170–172 | 140–142 | 106–108 | 220–222 | 138–140 | 160–162 | |
Time “min” | Con | 240 | 240 | 180 | 180 | 180 | 180 | 240 | 420 |
G | 10 | 12 | 14 | 17 | 16 | 13 | 11 | 14 | |
M.W | 2 | 2.5 | 2 | 4 | 3 | 2.5 | 3.5 | 3 | |
Yield % | Con | 80 | 75 | 78 | 76 | 76 | 75 | 81 | 85 |
G | 89.4 | 89.1 | 88.9 | 87.3 | 88.7 | 86.0 | 89.5 | 90.8 | |
M.W | 96.7 | 94.5 | 95.5 | 94.1 | 93.3 | 96.6 | 95.2 | 97.4 | |
YE | Con | 0.3333 | 0.3125 | 0.4333 | 0.4222 | 0.4222 | 0.4167 | 0.3375 | 0.2024 |
G | 8.94 | 7.43 | 6.35 | 5.14 | 5.54 | 6.62 | 7.50 | 6.49 | |
M.W | 48.35 | 37.80 | 47.75 | 23.53 | 31.10 | 38.64 | 27.20 | 32.47 | |
RME | Con | 66.19 | 62.62 | 58.78 | 67.66 | 60.60 | 58.93 | 73.16 | 66.27 |
G | 73.97 | 74.39 | 66.99 | 77.73 | 70.72 | 67.57 | 80.83 | 76.03 | |
M.W | 80.01 | 78.90 | 71.96 | 83.78 | 74.39 | 75.90 | 85.99 | 81.56 | |
OE | Con | 0.6619 | 0.6262 | 0.6562 | 0.7627 | 0.6400 | 0.6207 | 0.7634 | 0.6884 |
G | 0.7400 | 0.7439 | 0.7478 | 0.8762 | 0.7469 | 0.7117 | 0.8434 | 0.7898 | |
M.W | 0.8001 | 0.7890 | 0.8033 | 0.9444 | 0.7856 | 0.7995 | 0.8972 | 0.8473 | |
AE | 100 | 100 | 89.58 | 88.71 | 94.69 | 94.94 | 95.84 | 96.26 |