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Table 2 Analytical performance data for the determination of DRT, CAFF and PAR by the double divisor method

From: Smart green spectrophotometric assay of the ternary mixture of drotaverine, caffeine and paracetamol in their pharmaceutical dosage form

Parameter

DRT

CAFF

PAR

Wavelength (nm)

309 nm

288 nm

255 nm

Linearity range (µg/mL)

2–20

1.5–15

2–40

Intercept (a) × 10–3

− 8.360

0.0002

0.0147

Slope (b) × 10–3

22.164

0.016

0.026

Correlation coefficient (r)

0.9998

0.9999

0.9999

S.D. of residuals (Sy/x) × 10–3

2.72

0.001

0.004

S.D. of intercept (Sa) × 10–3

1.46

0.7 × 10–3

2 × 10–3

S.D. of slope (Sb) × 10–3

0.18

0.1 × 10–3

0.1 × 10–3

% RSDa

1.08

0.75

0.9

% Errorb

0.44

0.31

0.37

LODc (µg/mL)

0.22

0.14

0.24

LOQd (µg/mL)

0.66

0.42

0.71

  1. aPercentage relative standard deviation
  2. bPercentage relative error
  3. cLimits of detection
  4. dLimits of quantitation